Crystallography Open Database

Information card for entry 4121089

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Coordinates	4121089.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	rubidium germanium tridecaniobate
Formula	Ge Nb13 O60 Rb13
Calculated formula	Ge Nb12.99 O60.49 Rb13
Title of publication	Observing Assembly of Complex Inorganic Materials from Polyoxometalate Building Blocks
Authors of publication	Yu Hou; Lev N. Zakharov; May Nyman
Journal of publication	Journal of the American Chemical Society
Year of publication	2013
Journal volume	135
Pages of publication	16651 - 16657
a	13.849 ± 0.0016 Å
b	13.849 ± 0.0016 Å
c	19.84 ± 0.002 Å
α	90°
β	90°
γ	120°
Cell volume	3295.4 ± 0.6 Å³
Cell temperature	180 ± 2 K
Ambient diffraction temperature	180 ± 2 K
Number of distinct elements	4
Space group number	147
Hermann-Mauguin space group symbol	P -3
Hall space group symbol	-P 3
Residual factor for all reflections	0.0599
Residual factor for significantly intense reflections	0.0489
Weighted residual factors for significantly intense reflections	0.129
Weighted residual factors for all reflections included in the refinement	0.1383
Goodness-of-fit parameter for all reflections included in the refinement	1.065
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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