Crystallography Open Database

Information card for entry 4121627

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Coordinates	4121627.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H20 P2 S2
Calculated formula	C24 H20 P2 S2
Title of publication	Asymmetric synthesis of p-stereogenic diarylphosphinites by palladium-catalyzed enantioselective addition of diarylphosphines to benzoquinones.
Authors of publication	Huang, Yinhua; Li, Yongxin; Leung, Pak-Hing; Hayashi, Tamio
Journal of publication	Journal of the American Chemical Society
Year of publication	2014
Journal volume	136
Journal issue	13
Pages of publication	4865 - 4868
a	9.5656 ± 0.0005 Å
b	15.6505 ± 0.0009 Å
c	14.0777 ± 0.0008 Å
α	90°
β	96.8115 ± 0.0015°
γ	90°
Cell volume	2092.6 ± 0.2 Å³
Cell temperature	103 ± 2 K
Ambient diffraction temperature	103 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0784
Residual factor for significantly intense reflections	0.0487
Weighted residual factors for significantly intense reflections	0.1078
Weighted residual factors for all reflections included in the refinement	0.1237
Goodness-of-fit parameter for all reflections included in the refinement	1.123
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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