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Information card for entry 4121721
Preview
Coordinates | 4121721.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C47 H46 B F4 N5 P2 Rh |
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Calculated formula | C47 H46 B F4 N5 P2 Rh |
Title of publication | Intermolecular Hydroamination of 1,3-Dienes Catalyzed by Bis(phosphine)carbodicarbene-Rhodium Complexes. |
Authors of publication | Goldfogel, Matthew J.; Roberts, Courtney C.; Meek, Simon J. |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2014 |
Journal volume | 136 |
Journal issue | 17 |
Pages of publication | 6227 - 6230 |
a | 17.0682 ± 0.0004 Å |
b | 16.9409 ± 0.0004 Å |
c | 17.307 ± 0.0005 Å |
α | 90° |
β | 110.952 ± 0.001° |
γ | 90° |
Cell volume | 4673.4 ± 0.2 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100.15 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0437 |
Residual factor for significantly intense reflections | 0.0396 |
Weighted residual factors for significantly intense reflections | 0.1041 |
Weighted residual factors for all reflections included in the refinement | 0.1067 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.064 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4121721.html
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structural data.