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Information card for entry 4121739
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Coordinates | 4121739.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C23 H23 N O |
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Calculated formula | C23 H23 N O |
Title of publication | Mn-catalyzed three-component reactions of imines/nitriles, grignard reagents, and tetrahydrofuran: an expedient access to 1,5-amino/keto alcohols. |
Authors of publication | He, Ruoyu; Jin, Xiqing; Chen, Hui; Huang, Zhi-Tang; Zheng, Qi-Yu; Wang, Congyang |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2014 |
Journal volume | 136 |
Journal issue | 18 |
Pages of publication | 6558 - 6561 |
a | 9.814 ± 0.002 Å |
b | 5.6952 ± 0.0011 Å |
c | 16.213 ± 0.003 Å |
α | 90° |
β | 101.13 ± 0.03° |
γ | 90° |
Cell volume | 889.1 ± 0.3 Å3 |
Cell temperature | 173 ± 2 K |
Ambient diffraction temperature | 173 ± 2 K |
Number of distinct elements | 4 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0935 |
Residual factor for significantly intense reflections | 0.0783 |
Weighted residual factors for significantly intense reflections | 0.1257 |
Weighted residual factors for all reflections included in the refinement | 0.133 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.164 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4121739.html
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