Information card for entry 4121902

Structure parameters

• Formula: C32 H25 Cr3 N0 O12
• Calculated formula: C32 H29 Cr3 O11
• Title of publication: Stepwise Synthesis of Robust Metal-Organic Frameworks via Postsynthetic Metathesis and Oxidation of Metal Nodes in a Single-Crystal to Single-Crystal Transformation.
• Authors of publication: Liu, Tian-Fu; Zou, Lanfang; Feng, Dawei; Chen, Ying-Pin; Fordham, Stephen; Wang, Xuan; Liu, Yangyang; Zhou, Hong-Cai
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 22
• Pages of publication: 7813
• a: 40.881 ± 0.008 Å
• b: 40.881 ± 0.008 Å
• c: 40.881 ± 0.008 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 68323 ± 2 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 5
• Space group number: 225
• Hermann-Mauguin space group symbol: F m -3 m
• Hall space group symbol: -F 4 2 3
• Residual factor for all reflections: 0.3268
• Residual factor for significantly intense reflections: 0.1795
• Weighted residual factors for significantly intense reflections: 0.3935
• Weighted residual factors for all reflections included in the refinement: 0.4368
• Goodness-of-fit parameter for all reflections included in the refinement: 1.914
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No