Crystallography Open Database

Information card for entry 4121924

4121923 << 4121924 >> 4121925

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Coordinates	4121924.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C12 H42 Mo P4 Si
Calculated formula	C12 H42 Mo P4 Si
Title of publication	Si-H and Si-C Bond Cleavage Reactions of Silane and Phenylsilanes with Mo(PMe3)6: Silyl, Hypervalent Silyl, Silane, and Disilane Complexes.
Authors of publication	Zuzek, Ashley A.; Parkin, Gerard
Journal of publication	Journal of the American Chemical Society
Year of publication	2014
Journal volume	136
Journal issue	23
Pages of publication	8177 - 8180
a	13.8563 ± 0.0013 Å
b	13.5078 ± 0.0013 Å
c	12.344 ± 0.0012 Å
α	90°
β	90°
γ	90°
Cell volume	2310.4 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	36
Hermann-Mauguin space group symbol	C m c 21
Hall space group symbol	C 2c -2
Residual factor for all reflections	0.0421
Residual factor for significantly intense reflections	0.0318
Weighted residual factors for significantly intense reflections	0.0569
Weighted residual factors for all reflections included in the refinement	0.0604
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

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