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Information card for entry 4121967
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Coordinates | 4121967.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | cmpd5b |
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Formula | C46 H67 N O4 S4 Si4 |
Calculated formula | C44 H64 O4 S4 Si4 |
Title of publication | Dearomatization-induced transannular cyclization: synthesis of electron-accepting thiophene-s,s-dioxide-fused biphenylene. |
Authors of publication | Fukazawa, Aiko; Oshima, Hiroya; Shimizu, Soji; Kobayashi, Nagao; Yamaguchi, Shigehiro |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2014 |
Journal volume | 136 |
Journal issue | 24 |
Pages of publication | 8738 - 8745 |
a | 12.481 ± 0.007 Å |
b | 14.609 ± 0.007 Å |
c | 16.096 ± 0.008 Å |
α | 98.34 ± 0.02° |
β | 90.05 ± 0.02° |
γ | 108.281 ± 0.012° |
Cell volume | 2754 ± 2 Å3 |
Cell temperature | 123 ± 2 K |
Ambient diffraction temperature | 123 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0796 |
Residual factor for significantly intense reflections | 0.0648 |
Weighted residual factors for significantly intense reflections | 0.1754 |
Weighted residual factors for all reflections included in the refinement | 0.187 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.156 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4121967.html
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