Information card for entry 4122028

Structure parameters

• Formula: C35 H49 Al N2 O0.25 Si
• Calculated formula: C35 H49 Al N2 O0.25 Si
• Title of publication: Oxidative Addition of σ Bonds to an Al(I) Center.
• Authors of publication: Chu, Terry; Korobkov, Ilia; Nikonov, Georgii I.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 25
• Pages of publication: 9195 - 9202
• a: 9.633 ± 0.0005 Å
• b: 16.9749 ± 0.0008 Å
• c: 20.9503 ± 0.001 Å
• α: 90°
• β: 93.418 ± 0.003°
• γ: 90°
• Cell volume: 3419.7 ± 0.3 ų
• Cell temperature: 200 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0898
• Residual factor for significantly intense reflections: 0.0488
• Weighted residual factors for significantly intense reflections: 0.1168
• Weighted residual factors for all reflections included in the refinement: 0.1326
• Goodness-of-fit parameter for all reflections included in the refinement: 1.039
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No