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Information card for entry 4122093
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Coordinates | 4122093.cif |
---|---|
Original paper (by DOI) | HTML |
Common name | RhPh2(cod) Li(dme)3 |
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Chemical name | tris(1,2-dimethoxyethane)lithium (h4-1,5-cyclooctadiene)diphenylrhodate(I) |
Formula | C32 H52 Li O6 Rh |
Calculated formula | C32 H44 Li O6 Rh |
Title of publication | Diarylrhodates as promising active catalysts for the arylation of vinyl ethers with grignard reagents. |
Authors of publication | Iwasaki, Takanori; Miyata, Yoshinori; Akimoto, Ryo; Fujii, Yuuki; Kuniyasu, Hitoshi; Kambe, Nobuaki |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2014 |
Journal volume | 136 |
Journal issue | 26 |
Pages of publication | 9260 - 9263 |
a | 15.564 ± 0.004 Å |
b | 16.3801 ± 0.0016 Å |
c | 13.74 ± 0.008 Å |
α | 90° |
β | 109.64 ± 0.04° |
γ | 90° |
Cell volume | 3299 ± 2 Å3 |
Cell temperature | 123 K |
Ambient diffraction temperature | 123 K |
Number of distinct elements | 5 |
Space group number | 15 |
Hermann-Mauguin space group symbol | C 1 2/c 1 |
Hall space group symbol | -C 2yc |
Residual factor for significantly intense reflections | 0.0603 |
Weighted residual factors for all reflections included in the refinement | 0.1416 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.004 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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The link is: https://www.crystallography.net/4122093.html
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