Information card for entry 4122383

Structure parameters

• Formula: C25 H32 N2 O2
• Calculated formula: C25 H32 N2 O2
• SMILES: O=C(N1C2=C([C@]34N(CCC[C@@H]3[C@H](C2)C[C@H](C4)C)C(=O)c2ccccc2)CCC1)C
• Title of publication: Biogenetically inspired total syntheses of lycopodium alkaloids, (+)-flabellidine and (-)-lycodine.
• Authors of publication: Azuma, Masayuki; Yoshikawa, Tetsuya; Kogure, Noriyuki; Kitajima, Mariko; Takayama, Hiromitsu
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 33
• Pages of publication: 11618 - 11621
• a: 9.1575 ± 0.00017 Å
• b: 8.68997 ± 0.00016 Å
• c: 14.1387 ± 0.0003 Å
• α: 90°
• β: 110.322 ± 0.0008°
• γ: 90°
• Cell volume: 1055.1 ± 0.04 ų
• Cell temperature: 93 K
• Ambient diffraction temperature: 93 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for significantly intense reflections: 0.0437
• Weighted residual factors for all reflections included in the refinement: 0.1065
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 1.54187 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No