Information card for entry 4122498

Structure parameters

• Formula: Cl Fe3.5 H51.5 K5 Li6 O83.5 Si1.5 W15
• Calculated formula: Cl Fe3.16665 K5.05 O85.5 Si1.5 W15
• Title of publication: Controlling the minimal self assembly of "complex" polyoxometalate clusters.
• Authors of publication: Winter, Ross S.; Cameron, Jamie M.; Cronin, Leroy
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 36
• Pages of publication: 12753 - 12761
• a: 20.2088 ± 0.0008 Å
• b: 22.0401 ± 0.0006 Å
• c: 22.1265 ± 0.0009 Å
• α: 106.343 ± 0.003°
• β: 101.315 ± 0.003°
• γ: 109.851 ± 0.003°
• Cell volume: 8417.5 ± 0.6 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0875
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.0976
• Weighted residual factors for all reflections included in the refinement: 0.1167
• Goodness-of-fit parameter for all reflections included in the refinement: 1.03
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No