Information card for entry 4122680

Structure parameters

• Formula: C26.7 H23.4 F6 N3 O0.9 Pt Sb
• Calculated formula: C26.7 H23.4 F6 N3 O0.9 Pt Sb
• Title of publication: Oxygen Insertion into Metal Carbon Bonds: Formation of Methylperoxo Pd(II) and Pt(II) Complexes via Photogenerated Dinuclear Intermediates.
• Authors of publication: Petersen, Allan R.; Taylor, Russell A.; Vicente-Hernández, Inmaculada; Mallender, Philip R.; Olley, Harriet; White, Andrew J. P.; Britovsek, George J. P.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 40
• Pages of publication: 14089 - 14099
• a: 8.92385 ± 0.00016 Å
• b: 14.6411 ± 0.0003 Å
• c: 21.3047 ± 0.0003 Å
• α: 91.8823 ± 0.0015°
• β: 100.599 ± 0.0014°
• γ: 104.132 ± 0.0017°
• Cell volume: 2644.42 ± 0.09 ų
• Cell temperature: 173 K
• Ambient diffraction temperature: 173 K
• Number of distinct elements: 7
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.0427
• Residual factor for significantly intense reflections: 0.0338
• Weighted residual factors for significantly intense reflections: 0.0854
• Weighted residual factors for all reflections included in the refinement: 0.0871
• Goodness-of-fit parameter for all reflections included in the refinement: 1.079
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No