Information card for entry 4122726

Structure parameters

• Formula: C24 H35 Cl Ge N2 O3 W
• Calculated formula: C24 H35 Cl Ge N2 O3 W
• Title of publication: Cationic Metallogermylene and Dicationic Dimetallodigermenes: Synthesis by Chloride Abstraction from N-Heterocyclic Carbene-Stabilized Chlorometallogermylenes.
• Authors of publication: Inomata, Koya; Watanabe, Takahito; Tobita, Hiromi
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 41
• Pages of publication: 14341
• a: 16.7596 ± 0.0005 Å
• b: 9.4706 ± 0.0003 Å
• c: 17.3328 ± 0.0005 Å
• α: 90°
• β: 95.1602 ± 0.001°
• γ: 90°
• Cell volume: 2739.97 ± 0.14 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for all reflections: 0.068
• Residual factor for significantly intense reflections: 0.0544
• Weighted residual factors for significantly intense reflections: 0.1272
• Weighted residual factors for all reflections included in the refinement: 0.1358
• Goodness-of-fit parameter for all reflections included in the refinement: 1.197
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No