Information card for entry 4122728

Structure parameters

• Formula: C72 H63 B F24 Ge N2 O3 W
• Calculated formula: C72 H63 B F24 Ge N2 O3 W
• Title of publication: Cationic Metallogermylene and Dicationic Dimetallodigermenes: Synthesis by Chloride Abstraction from N-Heterocyclic Carbene-Stabilized Chlorometallogermylenes.
• Authors of publication: Inomata, Koya; Watanabe, Takahito; Tobita, Hiromi
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 41
• Pages of publication: 14341
• a: 14.9419 ± 0.0006 Å
• b: 18.725 ± 0.0006 Å
• c: 26.8623 ± 0.0009 Å
• α: 97.183 ± 0.0012°
• β: 92.0485 ± 0.001°
• γ: 101.438 ± 0.0009°
• Cell volume: 7294.5 ± 0.4 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1142
• Residual factor for significantly intense reflections: 0.0823
• Weighted residual factors for significantly intense reflections: 0.1989
• Weighted residual factors for all reflections included in the refinement: 0.2195
• Goodness-of-fit parameter for all reflections included in the refinement: 1.087
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No