Information card for entry 4122730

Structure parameters

• Formula: C104 H78 B2 F48 Ge2 N4 O6 W2
• Calculated formula: C104 H78 B2 F48 Ge2 N4 O6 W2
• Title of publication: Cationic Metallogermylene and Dicationic Dimetallodigermenes: Synthesis by Chloride Abstraction from N-Heterocyclic Carbene-Stabilized Chlorometallogermylenes.
• Authors of publication: Inomata, Koya; Watanabe, Takahito; Tobita, Hiromi
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2014
• Journal volume: 136
• Journal issue: 41
• Pages of publication: 14341
• a: 12.7478 ± 0.0012 Å
• b: 14.3085 ± 0.001 Å
• c: 16.6663 ± 0.0012 Å
• α: 111.179 ± 0.003°
• β: 99.6 ± 0.004°
• γ: 93.475 ± 0.003°
• Cell volume: 2770.7 ± 0.4 ų
• Cell temperature: 140 ± 2 K
• Ambient diffraction temperature: 140 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1062
• Residual factor for significantly intense reflections: 0.0842
• Weighted residual factors for significantly intense reflections: 0.2026
• Weighted residual factors for all reflections included in the refinement: 0.2149
• Goodness-of-fit parameter for all reflections included in the refinement: 1.199
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No