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Information card for entry 4122831
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Coordinates | 4122831.cif |
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Original paper (by DOI) | HTML |
Common name | NiCl2(CNArMes2)2 |
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Formula | C58.25 H59.375 Cl2 F1.125 N2 Ni O0.375 |
Calculated formula | C58.25 H59.375 Cl2 F1.125 N2 Ni O0.375 |
Title of publication | Direct Observation of β-Chloride Elimination from an Isolable β-Chloroalkyl Complex of Square-Planar Nickel. |
Authors of publication | Carpenter, Alex E.; McNeece, Andrew J.; Barnett, Brandon R.; Estrada, Alexander L.; Mokhtarzadeh, Charles C.; Moore, Curtis E.; Rheingold, Arnold L.; Perrin, Charles L.; Figueroa, Joshua S. |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2014 |
Journal volume | 136 |
Journal issue | 44 |
Pages of publication | 15481 - 15484 |
a | 12.3698 ± 0.001 Å |
b | 14.649 ± 0.0012 Å |
c | 16.2882 ± 0.0014 Å |
α | 69.508 ± 0.003° |
β | 70.124 ± 0.003° |
γ | 68.086 ± 0.003° |
Cell volume | 2489.4 ± 0.4 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 7 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0943 |
Residual factor for significantly intense reflections | 0.0473 |
Weighted residual factors for significantly intense reflections | 0.0918 |
Weighted residual factors for all reflections included in the refinement | 0.1055 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.003 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4122831.html
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Users of the data should acknowledge the original authors of the
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