Information card for entry 4123224

Structure parameters

• Common name: 4
• Formula: C30 H58 N3 O Si4 Y
• Calculated formula: C30 H58 N3 O Si4 Y
• Title of publication: Aminomethylation Reaction of ortho-Pyridyl C-H Bonds Catalyzed by Group 3 Metal Triamido Complexes.
• Authors of publication: Nagae, Haruki; Shibata, Yu; Tsurugi, Hayato; Mashima, Kazushi
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2015
• Journal volume: 137
• Journal issue: 2
• Pages of publication: 640 - 643
• a: 11.082 ± 0.006 Å
• b: 17.774 ± 0.009 Å
• c: 19.16 ± 0.01 Å
• α: 90°
• β: 93.361 ± 0.006°
• γ: 90°
• Cell volume: 3767 ± 3 ų
• Cell temperature: 113 ± 2 K
• Ambient diffraction temperature: 113 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0534
• Residual factor for significantly intense reflections: 0.0394
• Weighted residual factors for significantly intense reflections: 0.0873
• Weighted residual factors for all reflections included in the refinement: 0.0941
• Goodness-of-fit parameter for all reflections included in the refinement: 1.061
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No