Information card for entry 4123565

Structure parameters

• Common name: {(cAAC)Si(P-Tip)}2
• Formula: C172 H271 N4 P4 Si4
• Calculated formula: C172 H271 N4 P4 Si4
• Title of publication: Carbene supported dimer of heavier ketenimine analogue with p and si atoms.
• Authors of publication: Roy, Sudipta; Dittrich, Birger; Mondal, Totan; Koley, Debasis; Stückl, A Claudia; Schwederski, Brigitte; Kaim, Wolfgang; John, Michael; Vasa, Suresh Kumar; Linser, Rasmus; Roesky, Herbert W.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2015
• Journal volume: 137
• Journal issue: 19
• Pages of publication: 6180 - 6183
• a: 15.5998 ± 0.0006 Å
• b: 10.9274 ± 0.0005 Å
• c: 46.7138 ± 0.0019 Å
• α: 90°
• β: 93.599 ± 0.003°
• γ: 90°
• Cell volume: 7947.4 ± 0.6 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0778
• Residual factor for significantly intense reflections: 0.0495
• Weighted residual factors for significantly intense reflections: 0.0986
• Weighted residual factors for all reflections included in the refinement: 0.1097
• Goodness-of-fit parameter for all reflections included in the refinement: 1.026
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No