Total Syntheses of (-)-Mersicarpine, (-)-Scholarisine G, (+)-Melodinine E, (-)-Leuconoxine, (-)-Leuconolam, (-)-Leuconodine A, (+)-Leuconodine F, and (-)-Leuconodine C: Self-Induced Diastereomeric Anisochronism (SIDA) Phenomenon for Scholarisine G and Leuconodines A and C.
Authors of publication
Xu, Zhengren; Wang, Qian; Zhu, Jieping
Journal of publication
Journal of the American Chemical Society
Year of publication
2015
Journal volume
137
Journal issue
20
Pages of publication
6712 - 6724
a
6.7177 ± 0.0007 Å
b
27.31 ± 0.003 Å
c
11.8448 ± 0.0009 Å
α
90°
β
99.883 ± 0.007°
γ
90°
Cell volume
2140.8 ± 0.4 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100 ± 2 K
Number of distinct elements
4
Space group number
14
Hermann-Mauguin space group symbol
P 1 21/c 1
Hall space group symbol
-P 2ybc
Residual factor for all reflections
0.0727
Residual factor for significantly intense reflections
0.0579
Weighted residual factors for significantly intense reflections
0.1299
Weighted residual factors for all reflections included in the refinement
0.139
Goodness-of-fit parameter for all reflections included in the refinement
