Information card for entry 4123649

Structure parameters

• Formula: C73 H52 B F24 N4 P2 Rh
• Calculated formula: C73 H51.198 B F23.894 N4 P2 Rh
• Title of publication: Lewis Acid activation of carbodicarbene catalysts for rh-catalyzed hydroarylation of dienes.
• Authors of publication: Roberts, Courtney C.; Matías, Desirée M; Goldfogel, Matthew J.; Meek, Simon J.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2015
• Journal volume: 137
• Journal issue: 20
• Pages of publication: 6488 - 6491
• a: 14.5732 ± 0.0005 Å
• b: 16.2543 ± 0.0006 Å
• c: 16.4636 ± 0.0006 Å
• α: 72.9946 ± 0.0016°
• β: 69.1536 ± 0.0017°
• γ: 78.171 ± 0.0016°
• Cell volume: 3462.9 ± 0.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100.15 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0352
• Residual factor for significantly intense reflections: 0.0336
• Weighted residual factors for significantly intense reflections: 0.1117
• Weighted residual factors for all reflections included in the refinement: 0.1139
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No