Information card for entry 4123839

Structure parameters

• Formula: C43 H52 O5 Si
• Calculated formula: C43 H52 O5 Si
• Title of publication: Asymmetric Annulation of Donor-Acceptor Cyclopropanes with Dienes.
• Authors of publication: Xu, Hao; Hu, Jiang-Lin; Wang, Lijia; Liao, Saihu; Tang, Yong
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2015
• Journal volume: 137
• Journal issue: 25
• Pages of publication: 8006 - 8009
• a: 17.8087 ± 0.0017 Å
• b: 9.8394 ± 0.001 Å
• c: 23.122 ± 0.002 Å
• α: 90°
• β: 111.454 ± 0.002°
• γ: 90°
• Cell volume: 3770.9 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1491
• Residual factor for significantly intense reflections: 0.0847
• Weighted residual factors for significantly intense reflections: 0.212
• Weighted residual factors for all reflections included in the refinement: 0.2528
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No