Ligand Aspect Ratio as a Decisive Factor for the Self-Assembly of Coordination Cages.
Authors of publication
Jansze, Suzanne M.; Cecot, Giacomo; Wise, Matthew D.; Zhurov, Konstantin O.; Ronson, Tanya K.; Castilla, Ana M.; Finelli, Alba; Pattison, Philip; Solari, Euro; Scopelliti, Rosario; Zelinskii, Genrikh E.; Vologzhanina, Anna V.; Voloshin, Yan Z.; Nitschke, Jonathan R.; Severin, Kay
Journal of publication
Journal of the American Chemical Society
Year of publication
2016
Journal volume
138
Journal issue
6
Pages of publication
2046 - 2054
a
24.958 ± 0.003 Å
b
8.872 ± 0.0013 Å
c
16.619 ± 0.002 Å
α
90°
β
98.044 ± 0.016°
γ
90°
Cell volume
3643.7 ± 0.8 Å3
Cell temperature
100 ± 2 K
Ambient diffraction temperature
100.15 K
Number of distinct elements
6
Space group number
15
Hermann-Mauguin space group symbol
C 1 2/c 1
Hall space group symbol
-C 2yc
Residual factor for all reflections
0.1048
Residual factor for significantly intense reflections
0.0929
Weighted residual factors for significantly intense reflections
0.215
Weighted residual factors for all reflections included in the refinement
0.2207
Goodness-of-fit parameter for all reflections included in the refinement
