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Information card for entry 4124937
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Coordinates | 4124937.cif |
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Original paper (by DOI) | HTML |
Formula | C28 H59 Lu O Si4 |
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Calculated formula | C28 H59 Lu O Si4 |
Title of publication | The Nature of Secondary Interactions at Electrophilic Metal Sites of Molecular and Silica-Supported Organolutetium Complexes from Solid-State NMR Spectroscopy. |
Authors of publication | Conley, Matthew P.; Lapadula, Giuseppe; Sanders, Kevin; Gajan, David; Lesage, Anne; Del Rosal, Iker; Maron, Laurent; Lukens, Wayne W.; Copéret, Christophe; Andersen, Richard A. |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2016 |
Journal volume | 138 |
Journal issue | 11 |
Pages of publication | 3831 - 3843 |
a | 12.802 ± 0.0015 Å |
b | 13.5388 ± 0.0015 Å |
c | 20.551 ± 0.002 Å |
α | 89.663 ± 0.004° |
β | 89.314 ± 0.003° |
γ | 89.923 ± 0.003° |
Cell volume | 3561.7 ± 0.7 Å3 |
Cell temperature | 100 K |
Ambient diffraction temperature | 100 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.1059 |
Residual factor for significantly intense reflections | 0.0801 |
Weighted residual factors for significantly intense reflections | 0.1761 |
Weighted residual factors for all reflections included in the refinement | 0.1925 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.198 |
Diffraction radiation probe | x-ray |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
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