The Nature of Secondary Interactions at Electrophilic Metal Sites of Molecular and Silica-Supported Organolutetium Complexes from Solid-State NMR Spectroscopy.
Authors of publication
Conley, Matthew P.; Lapadula, Giuseppe; Sanders, Kevin; Gajan, David; Lesage, Anne; Del Rosal, Iker; Maron, Laurent; Lukens, Wayne W.; Copéret, Christophe; Andersen, Richard A.
Journal of publication
Journal of the American Chemical Society
Year of publication
2016
Journal volume
138
Journal issue
11
Pages of publication
3831 - 3843
a
12.6449 ± 0.001 Å
b
14.338 ± 0.0011 Å
c
22.5972 ± 0.0018 Å
α
69.3403 ± 0.0014°
β
77.9753 ± 0.0014°
γ
89.5638 ± 0.0014°
Cell volume
3739.6 ± 0.5 Å3
Cell temperature
100 K
Ambient diffraction temperature
100 K
Number of distinct elements
5
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0665
Residual factor for significantly intense reflections
0.0427
Weighted residual factors for significantly intense reflections
0.0899
Weighted residual factors for all reflections included in the refinement
0.0989
Goodness-of-fit parameter for all reflections included in the refinement
