Information card for entry 4125007

Structure parameters

• Chemical name: Sn{B(NArCH)2}2(OH)(H)
• Formula: C52 H74 B2 N4 O Sn
• Calculated formula: C52 H74 B2 N4 O Sn
• Title of publication: Enabling and Probing Oxidative Addition and Reductive Elimination at a Group 14 Metal Center: Cleavage and Functionalization of E-H Bonds by a Bis(boryl)stannylene.
• Authors of publication: Protchenko, Andrey V.; Bates, Joshua I.; Saleh, Liban M. A.; Blake, Matthew P.; Schwarz, Andrew D.; Kolychev, Eugene L.; Thompson, Amber L.; Jones, Cameron; Mountford, Philip; Aldridge, Simon
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 13
• Pages of publication: 4555 - 4564
• a: 21.22087 ± 0.00016 Å
• b: 12.54026 ± 0.00011 Å
• c: 19.63737 ± 0.00017 Å
• α: 90°
• β: 97.8858 ± 0.0008°
• γ: 90°
• Cell volume: 5176.39 ± 0.08 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.05
• Residual factor for significantly intense reflections: 0.0491
• Weighted residual factors for all reflections: 0.0464
• Weighted residual factors for significantly intense reflections: 0.0461
• Weighted residual factors for all reflections included in the refinement: 0.0459
• Goodness-of-fit parameter for all reflections included in the refinement: 1.1057
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No