Information card for entry 4125010

Structure parameters

• Formula: C55 H77 B2 K N5 Sn
• Calculated formula: C55 H77 B2 K N5 Sn
• Title of publication: Enabling and Probing Oxidative Addition and Reductive Elimination at a Group 14 Metal Center: Cleavage and Functionalization of E-H Bonds by a Bis(boryl)stannylene.
• Authors of publication: Protchenko, Andrey V.; Bates, Joshua I.; Saleh, Liban M. A.; Blake, Matthew P.; Schwarz, Andrew D.; Kolychev, Eugene L.; Thompson, Amber L.; Jones, Cameron; Mountford, Philip; Aldridge, Simon
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 13
• Pages of publication: 4555 - 4564
• a: 17.8585 ± 0.0001 Å
• b: 43.5512 ± 0.0002 Å
• c: 19.1937 ± 0.0001 Å
• α: 90°
• β: 117.11 ± 0.0003°
• γ: 90°
• Cell volume: 13288 ± 0.12 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/a 1
• Hall space group symbol: -P 2yab
• Residual factor for all reflections: 0.0941
• Residual factor for significantly intense reflections: 0.0576
• Weighted residual factors for all reflections: 0.1812
• Weighted residual factors for significantly intense reflections: 0.1433
• Weighted residual factors for all reflections included in the refinement: 0.1812
• Goodness-of-fit parameter for all reflections included in the refinement: 0.9674
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No