Information card for entry 4125195

Structure parameters

• Formula: C34 H54 B Li N4 O
• Calculated formula: C34 H54 B Li N4 O
• Title of publication: Alkali Metal Hydridotriphenylborates [(L)M][HBPh3] (M = Li, Na, K): Chemoselective Catalysts for Carbonyl and CO2 Hydroboration.
• Authors of publication: Mukherjee, Debabrata; Osseili, Hassan; Spaniol, Thomas P.; Okuda, Jun
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 34
• Pages of publication: 10790 - 10793
• a: 11.97 ± 0.002 Å
• b: 12.297 ± 0.002 Å
• c: 17.763 ± 0.003 Å
• α: 80.063 ± 0.005°
• β: 76.452 ± 0.005°
• γ: 82.123 ± 0.006°
• Cell volume: 2491 ± 0.7 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 6
• Space group number: 1
• Hermann-Mauguin space group symbol: P 1
• Hall space group symbol: P 1
• Residual factor for all reflections: 0.1638
• Residual factor for significantly intense reflections: 0.0873
• Weighted residual factors for significantly intense reflections: 0.1739
• Weighted residual factors for all reflections included in the refinement: 0.2179
• Goodness-of-fit parameter for all reflections included in the refinement: 1.016
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No