Information card for entry 4125247

Structure parameters

• Formula: C39 H49 F5 Mg N2 O
• Calculated formula: C39 H49 F5 Mg N2 O
• Title of publication: Addition of Carbon-Fluorine Bonds to a Mg(I)-Mg(I) Bond: An Equivalent of Grignard Formation in Solution.
• Authors of publication: Bakewell, Clare; White, Andrew J. P.; Crimmin, Mark R.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 39
• Pages of publication: 12763 - 12766
• a: 12.8601 ± 0.0011 Å
• b: 15.9403 ± 0.0014 Å
• c: 18.1538 ± 0.0013 Å
• α: 84.244 ± 0.007°
• β: 89.38 ± 0.006°
• γ: 88.675 ± 0.007°
• Cell volume: 3701.5 ± 0.5 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1694
• Residual factor for significantly intense reflections: 0.0715
• Weighted residual factors for significantly intense reflections: 0.1904
• Weighted residual factors for all reflections included in the refinement: 0.2208
• Goodness-of-fit parameter for all reflections included in the refinement: 0.813
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No