Information card for entry 4125321

Structure parameters

• Common name: (Ph3CO)4(DME)U
• Chemical name: Tetrakis(triphenylmethoxy) uranium(IV) DME adduct
• Formula: C80 H70 O6 U
• Calculated formula: C80 H70 O6 U
• Title of publication: A Homoleptic Uranium(III) Tris(aryl) Complex.
• Authors of publication: Boreen, Michael A.; Parker, Bernard F.; Lohrey, Trevor D.; Arnold, John
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 49
• Pages of publication: 15865 - 15868
• a: 13.5754 ± 0.0009 Å
• b: 20.2128 ± 0.0013 Å
• c: 22.6448 ± 0.0014 Å
• α: 90°
• β: 98.582 ± 0.003°
• γ: 90°
• Cell volume: 6144.1 ± 0.7 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0235
• Residual factor for significantly intense reflections: 0.0195
• Weighted residual factors for significantly intense reflections: 0.0461
• Weighted residual factors for all reflections included in the refinement: 0.0476
• Goodness-of-fit parameter for all reflections included in the refinement: 1.054
• Diffraction radiation wavelength: 0.7749 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No