Information card for entry 4125754

Structure parameters

• Common name: Pd-complex
• Chemical name: Pd-complex
• Formula: C28 H29 N3 O6 Pd S
• Calculated formula: C28 H29 N3 O6 Pd S
• Title of publication: Reductive C(sp(2))-N Elimination from Isolated Pd(IV) Amido Aryl Complexes Prepared Using H2O2 as Oxidant.
• Authors of publication: Abada, Elikplim; Zavalij, Peter Y.; Vedernikov, Andrei N.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2017
• Journal volume: 139
• Journal issue: 2
• Pages of publication: 643 - 646
• a: 30.3195 ± 0.0017 Å
• b: 11.3339 ± 0.0006 Å
• c: 17.6574 ± 0.001 Å
• α: 90°
• β: 118.758 ± 0.0008°
• γ: 90°
• Cell volume: 5319.4 ± 0.5 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 6
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0438
• Residual factor for significantly intense reflections: 0.0336
• Weighted residual factors for significantly intense reflections: 0.0659
• Weighted residual factors for all reflections included in the refinement: 0.0685
• Goodness-of-fit parameter for all reflections included in the refinement: 1.387
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No