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Information card for entry 4125770
Preview
Coordinates | 4125770.cif |
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Original paper (by DOI) | HTML |
Formula | C41 H50 Cl2 N4 O6 S2 |
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Calculated formula | C41 H50 Cl2 N4 O6 S2 |
Title of publication | Functional-Group-Tolerant, Silver-Catalyzed N-N Bond Formation by Nitrene Transfer to Amines. |
Authors of publication | Maestre, Lourdes; Dorel, Ruth; Pablo, Óscar; Escofet, Imma; Sameera, W. M. C.; Álvarez, Eleuterio; Maseras, Feliu; Díaz-Requejo, M Mar; Echavarren, Antonio M.; Pérez, Pedro J |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2017 |
Journal volume | 139 |
Journal issue | 6 |
Pages of publication | 2216 - 2223 |
a | 7.3139 ± 0.0006 Å |
b | 11.178 ± 0.001 Å |
c | 12.6984 ± 0.001 Å |
α | 76.605 ± 0.005° |
β | 86.384 ± 0.007° |
γ | 85.863 ± 0.008° |
Cell volume | 1006.13 ± 0.15 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.0394 |
Residual factor for significantly intense reflections | 0.0343 |
Weighted residual factors for significantly intense reflections | 0.0891 |
Weighted residual factors for all reflections included in the refinement | 0.0919 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.033 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4125770.html
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