Crystallography Open Database

Information card for entry 4125897

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Coordinates	4125897.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C40 H80 Li4 O4 Pd Si4
Calculated formula	C40 H80 Li4 O4 Pd Si4
Title of publication	Spiro Metallaaromatics of Pd, Pt, Rh: Synthesis and Characterization.
Authors of publication	Zhang, Yongliang; Wei, Junnian; Chi, Yue; Zhang, Xuan; Zhang, Wen-Xiong; Xi, Zhenfeng
Journal of publication	Journal of the American Chemical Society
Year of publication	2017
a	11.8364 ± 0.0003 Å
b	20.54 ± 0.0006 Å
c	20.7869 ± 0.0006 Å
α	90°
β	94.764 ± 0.003°
γ	90°
Cell volume	5036.2 ± 0.2 Å³
Cell temperature	180 ± 0.1 K
Ambient diffraction temperature	180 ± 0.1 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0448
Residual factor for significantly intense reflections	0.0322
Weighted residual factors for significantly intense reflections	0.0702
Weighted residual factors for all reflections included in the refinement	0.0764
Goodness-of-fit parameter for all reflections included in the refinement	1.053
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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