Information card for entry 4126116

Structure parameters

• Formula: C39 H57 Pb
• Calculated formula: C39 H57 Pb
• Title of publication: Low-Valent Lead Hydride and Its Extreme Low-Field (1)H NMR Chemical Shift.
• Authors of publication: Schneider, Julia; Sindlinger, Christian P.; Eichele, Klaus; Schubert, Hartmut; Wesemann, Lars
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2017
• Journal volume: 139
• Journal issue: 19
• Pages of publication: 6542 - 6545
• a: 13.2953 ± 0.0003 Å
• b: 15.9523 ± 0.0004 Å
• c: 16.985 ± 0.0004 Å
• α: 90°
• β: 104.356 ± 0.001°
• γ: 90°
• Cell volume: 3489.87 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 3
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0444
• Residual factor for significantly intense reflections: 0.0282
• Weighted residual factors for significantly intense reflections: 0.0572
• Weighted residual factors for all reflections included in the refinement: 0.0616
• Goodness-of-fit parameter for all reflections included in the refinement: 1.018
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No