Information card for entry 4127011

Structure parameters

• Formula: C70.38 H40.58 Dy3 F36.19 N18 O13.12
• Calculated formula: C70.093 H40.083 Dy3 F36.078 N18 O13.033
• Title of publication: Lanthanide Triangles Supported by Radical Bridging Ligands.
• Authors of publication: Dolinar, Brian S.; Alexandropoulos, Dimitris I.; Vignesh, Kuduva R.; James, Tia'Asia; Dunbar, Kim R.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2017
• a: 14.8664 ± 0.0008 Å
• b: 16.6091 ± 0.0009 Å
• c: 19.8643 ± 0.001 Å
• α: 73.227 ± 0.003°
• β: 78.36 ± 0.003°
• γ: 79.675 ± 0.004°
• Cell volume: 4561.1 ± 0.4 ų
• Cell temperature: 110 K
• Ambient diffraction temperature: 110 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1298
• Residual factor for significantly intense reflections: 0.059
• Weighted residual factors for significantly intense reflections: 0.0989
• Weighted residual factors for all reflections included in the refinement: 0.1245
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Diffraction radiation X-ray symbol: K-L~3~
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No