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Information card for entry 4127063
Preview
Coordinates | 4127063.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C62 H52 B F24 O P2 Rh |
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Calculated formula | C62 H52 B F24 O P2 Rh |
Title of publication | Dehydropolymerization of H3B·NMeH2 To Form Polyaminoboranes Using [Rh(Xantphos-alkyl)] Catalysts. |
Authors of publication | Adams, Gemma M.; Colebatch, Annie L.; Skornia, Joseph T.; McKay, Alasdair I.; Johnson, Heather C.; Lloyd Jones, Guy C.; Macgregor, Stuart A.; Beattie, Nicholas A.; Weller, Andrew S. |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2018 |
a | 18.6622 ± 0.0002 Å |
b | 17.9481 ± 0.0002 Å |
c | 19.1933 ± 0.0003 Å |
α | 90° |
β | 102.159 ± 0.0013° |
γ | 90° |
Cell volume | 6284.59 ± 0.14 Å3 |
Cell temperature | 150 K |
Ambient diffraction temperature | 150 K |
Number of distinct elements | 7 |
Space group number | 14 |
Hermann-Mauguin space group symbol | P 1 21/c 1 |
Hall space group symbol | -P 2ybc |
Residual factor for all reflections | 0.0676 |
Residual factor for significantly intense reflections | 0.0621 |
Weighted residual factors for all reflections | 0.1601 |
Weighted residual factors for significantly intense reflections | 0.1507 |
Weighted residual factors for all reflections included in the refinement | 0.1601 |
Goodness-of-fit parameter for all reflections included in the refinement | 0.9583 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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The link is: https://www.crystallography.net/4127063.html
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