Information card for entry 4127069

Structure parameters

• Formula: C31 H61 B3 Cl2 Ge N O P2 Si2
• Calculated formula: C31 H61 B3 Cl2 Ge N O P2 Si2
• Title of publication: A Boron Analogue of Vinylidene Dication Supported by Phosphines.
• Authors of publication: Lu, Wei; Li, Yongxin; Ganguly, Rakesh; Kinjo, Rei
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• a: 15.6607 ± 0.0004 Å
• b: 14.8784 ± 0.0005 Å
• c: 36.9796 ± 0.0012 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 8616.5 ± 0.5 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 9
• Space group number: 29
• Hermann-Mauguin space group symbol: P c a 21
• Hall space group symbol: P 2c -2ac
• Residual factor for all reflections: 0.0672
• Residual factor for significantly intense reflections: 0.0436
• Weighted residual factors for significantly intense reflections: 0.0834
• Weighted residual factors for all reflections included in the refinement: 0.0941
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No