Information card for entry 4127177

Structure parameters

• Formula: C28 H46 Ge Hf Si2
• Calculated formula: C28 H46 Ge Hf Si2
• Title of publication: Hafnocene-based Bicyclo[2.1.1]hexene Germylenes - Formation, Reactivity and Structural Flexibility.
• Authors of publication: Dong, Zhaowen; Bedbur, Katja; Schmidtmann, Marc; Müller, Thomas
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2018
• a: 8.1141 ± 0.0003 Å
• b: 22.8961 ± 0.0007 Å
• c: 16.1407 ± 0.0005 Å
• α: 90°
• β: 95.5255 ± 0.0014°
• γ: 90°
• Cell volume: 2984.71 ± 0.17 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0378
• Residual factor for significantly intense reflections: 0.0317
• Weighted residual factors for significantly intense reflections: 0.07
• Weighted residual factors for all reflections included in the refinement: 0.0724
• Goodness-of-fit parameter for all reflections included in the refinement: 1.164
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No