Information card for entry 4127693

Structure parameters

• Formula: C172 H230 Cl12 N4 O36 Rh8
• Calculated formula: C172 H230 Cl12 N4 O36 Rh8
• Title of publication: Characterization of a Reactive Rh₂ Nitrenoid by Crystalline Matrix Isolation.
• Authors of publication: Das, Anuvab; Chen, Yu-Sheng; Reibenspies, Joseph H.; Powers, David C.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• Journal volume: 141
• Journal issue: 41
• Pages of publication: 16232 - 16236
• a: 19.6255 ± 0.001 Å
• b: 21.4629 ± 0.001 Å
• c: 22.5422 ± 0.0011 Å
• α: 90°
• β: 109.875 ± 0.002°
• γ: 90°
• Cell volume: 8929.7 ± 0.8 ų
• Cell temperature: 110 ± 2 K
• Ambient diffraction temperature: 110 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0729
• Residual factor for significantly intense reflections: 0.0541
• Weighted residual factors for significantly intense reflections: 0.096
• Weighted residual factors for all reflections included in the refinement: 0.1024
• Goodness-of-fit parameter for all reflections included in the refinement: 1.154
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No