Information card for entry 4127695

Structure parameters

• Formula: C54 H74 Cl4 N6 O8 Rh2
• Calculated formula: C54 H74 Cl4 N6 O8 Rh2
• Title of publication: Characterization of a Reactive Rh₂ Nitrenoid by Crystalline Matrix Isolation.
• Authors of publication: Das, Anuvab; Chen, Yu-Sheng; Reibenspies, Joseph H.; Powers, David C.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• Journal volume: 141
• Journal issue: 41
• Pages of publication: 16232 - 16236
• a: 11.0301 ± 0.0019 Å
• b: 14.251 ± 0.002 Å
• c: 18.763 ± 0.003 Å
• α: 90°
• β: 107.025 ± 0.002°
• γ: 90°
• Cell volume: 2820.1 ± 0.8 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0676
• Residual factor for significantly intense reflections: 0.0481
• Weighted residual factors for significantly intense reflections: 0.123
• Weighted residual factors for all reflections included in the refinement: 0.135
• Goodness-of-fit parameter for all reflections included in the refinement: 1.023
• Diffraction radiation probe: x-ray
• Diffraction radiation wavelength: 0.33062 Å
• Diffraction radiation type: synchrotron
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No