Information card for entry 4127796

Structure parameters

• Formula: C65 H78 Ge2 P2
• Calculated formula: C65 H78 Ge2 P2
• SMILES: [Ge@]12([Ge]([P](c3c2cccc3)(c2ccccc2)c2ccccc2)C(=P1)C12CC3CC(CC(C3)C1)C2)c1c(cccc1c1c(C(C)C)cc(C(C)C)cc1C(C)C)c1c(cc(C(C)C)cc1C(C)C)C(C)C
• Title of publication: Phosphine-Stabilized Digermavinylidene.
• Authors of publication: Krebs, Kilian M.; Hanselmann, Dominik; Schubert, Hartmut; Wurst, Kai; Scheele, Marcus; Wesemann, Lars
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• Journal volume: 141
• Journal issue: 8
• Pages of publication: 3424 - 3429
• a: 10.8251 ± 0.0004 Å
• b: 28.5433 ± 0.001 Å
• c: 18.1586 ± 0.0006 Å
• α: 90°
• β: 91.12 ± 0.002°
• γ: 90°
• Cell volume: 5609.6 ± 0.3 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 4
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0895
• Residual factor for significantly intense reflections: 0.0581
• Weighted residual factors for significantly intense reflections: 0.1002
• Weighted residual factors for all reflections included in the refinement: 0.1117
• Goodness-of-fit parameter for all reflections included in the refinement: 1.067
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No