Information card for entry 4128307

Structure parameters

• Formula: C79.5 H54 B Cl F24 O P2 Pd
• Calculated formula: C79.5 H54 B Cl F24 O P2 Pd
• Title of publication: Silylpalladium Cations Enable the Oxidative Addition of C(sp³)-O Bonds.
• Authors of publication: Wierschen, Andreas L.; Romano, Neyen; Lee, Stephen J.; Gagné, Michel R
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• Journal volume: 141
• Journal issue: 40
• Pages of publication: 16024 - 16032
• a: 14.6401 ± 0.0003 Å
• b: 17.2051 ± 0.0004 Å
• c: 17.93 ± 0.0004 Å
• α: 115.267 ± 0.0013°
• β: 96.9948 ± 0.0016°
• γ: 103.786 ± 0.0018°
• Cell volume: 3836 ± 0.17 ų
• Cell temperature: 150 K
• Ambient diffraction temperature: 150 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0751
• Residual factor for significantly intense reflections: 0.0658
• Weighted residual factors for all reflections: 0.1781
• Weighted residual factors for significantly intense reflections: 0.1709
• Weighted residual factors for all reflections included in the refinement: 0.1781
• Goodness-of-fit parameter for all reflections included in the refinement: 1.0248
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No