Information card for entry 4128327

Structure parameters

• Formula: C229 H96 Au24 Cl2 F108 P2 Pt
• Calculated formula: C229 H96 Au24 Cl2 F108 P2 Pt
• Title of publication: Efficient and Selective Conversion of Phosphine-Protected (MAu₈)²⁺ (M = Pd, Pt) Superatoms to Thiolate-Protected (MAu₁₂)⁶⁺ or Alkynyl-Protected (MAu₁₂)⁴⁺ Superatoms via Hydride Doping.
• Authors of publication: Takano, Shinjiro; Ito, Shun; Tsukuda, Tatsuya
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2019
• Journal volume: 141
• Journal issue: 40
• Pages of publication: 15994 - 16002
• a: 17.464 ± 0.003 Å
• b: 20.626 ± 0.004 Å
• c: 35.907 ± 0.007 Å
• α: 90°
• β: 95.69 ± 0.003°
• γ: 90°
• Cell volume: 12870 ± 4 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 7
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.0699
• Residual factor for significantly intense reflections: 0.0627
• Weighted residual factors for significantly intense reflections: 0.1612
• Weighted residual factors for all reflections included in the refinement: 0.1668
• Goodness-of-fit parameter for all reflections included in the refinement: 1.122
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No