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Information card for entry 4128332
Preview
Coordinates | 4128332.cif |
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Original paper (by DOI) | HTML |
Formula | C229 H96 Au24 Cl2 F108 P2 Pd |
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Calculated formula | C229 H96 Au24 Cl2 F108 P2 Pd |
Title of publication | Efficient and Selective Conversion of Phosphine-Protected (MAu<sub>8</sub>)<sup>2+</sup> (M = Pd, Pt) Superatoms to Thiolate-Protected (MAu<sub>12</sub>)<sup>6+</sup> or Alkynyl-Protected (MAu<sub>12</sub>)<sup>4+</sup> Superatoms via Hydride Doping. |
Authors of publication | Takano, Shinjiro; Ito, Shun; Tsukuda, Tatsuya |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2019 |
Journal volume | 141 |
Journal issue | 40 |
Pages of publication | 15994 - 16002 |
a | 17.477 ± 0.004 Å |
b | 20.733 ± 0.004 Å |
c | 35.724 ± 0.007 Å |
α | 90° |
β | 95.792 ± 0.003° |
γ | 90° |
Cell volume | 12879 ± 5 Å3 |
Cell temperature | 93 ± 2 K |
Ambient diffraction temperature | 93 ± 2 K |
Number of distinct elements | 7 |
Space group number | 13 |
Hermann-Mauguin space group symbol | P 1 2/n 1 |
Hall space group symbol | -P 2yac |
Residual factor for all reflections | 0.0725 |
Residual factor for significantly intense reflections | 0.0633 |
Weighted residual factors for significantly intense reflections | 0.1563 |
Weighted residual factors for all reflections included in the refinement | 0.1632 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.124 |
Diffraction radiation wavelength | 0.71075 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
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