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Information card for entry 4128757
Preview
Coordinates | 4128757.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H43 N O3 Si |
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Calculated formula | C27 H43 N O3 Si |
SMILES | C1C(=O)C=C2[C@@H]1CC[C@H]1[C@H]2N2C[C@@H](C)[C@H]3CC[C@]([C@@H]23)(C1=O)CCCO[Si](C)(C)C(C)(C)C |
Title of publication | Calyciphylline B-Type Alkaloids: Total Syntheses of (-)-Daphlongamine H and (-)-Isodaphlongamine H. |
Authors of publication | Hugelshofer, Cedric L.; Palani, Vignesh; Sarpong, Richmond |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2019 |
Journal volume | 141 |
Journal issue | 21 |
Pages of publication | 8431 - 8435 |
a | 8.19798 ± 0.00005 Å |
b | 7.89375 ± 0.00004 Å |
c | 20.23662 ± 0.0001 Å |
α | 90° |
β | 99.2147 ± 0.0005° |
γ | 90° |
Cell volume | 1292.67 ± 0.012 Å3 |
Cell temperature | 100 ± 2 K |
Ambient diffraction temperature | 100 ± 2 K |
Number of distinct elements | 5 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.0559 |
Residual factor for significantly intense reflections | 0.0556 |
Weighted residual factors for significantly intense reflections | 0.1517 |
Weighted residual factors for all reflections included in the refinement | 0.152 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.043 |
Diffraction radiation wavelength | 1.54184 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4128757.html
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