Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4128933
Preview
Coordinates | 4128933.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C33 H42 N2 O2 Si |
---|---|
Calculated formula | C33 H42 N2 O2 Si |
Title of publication | Pd(II)-Catalyzed Enantioselective Alkynylation of Unbiased Methylene C(sp<sup>3</sup>)-H Bonds Using 3,3'-Fluorinated-BINOL as a Chiral Ligand. |
Authors of publication | Han, Ye-Qiang; Ding, Yi; Zhou, Tao; Yan, Sheng-Yi; Song, Hong; Shi, Bing-Feng |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2019 |
Journal volume | 141 |
Journal issue | 11 |
Pages of publication | 4558 - 4563 |
a | 25.919 ± 0.0011 Å |
b | 9.9765 ± 0.0004 Å |
c | 26.3509 ± 0.0011 Å |
α | 90° |
β | 112.699 ± 0.002° |
γ | 90° |
Cell volume | 6286.1 ± 0.5 Å3 |
Cell temperature | 170 ± 2 K |
Ambient diffraction temperature | 170 K |
Number of distinct elements | 5 |
Space group number | 4 |
Hermann-Mauguin space group symbol | P 1 21 1 |
Hall space group symbol | P 2yb |
Residual factor for all reflections | 0.1056 |
Residual factor for significantly intense reflections | 0.1016 |
Weighted residual factors for significantly intense reflections | 0.293 |
Weighted residual factors for all reflections included in the refinement | 0.3039 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.381 |
Diffraction radiation wavelength | 1.54178 Å |
Diffraction radiation type | CuKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4128933.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.