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Information card for entry 4129019
Preview
Coordinates | 4129019.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C27 H43.44 N3 Si3 V |
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Calculated formula | C27 H43.45 N3 Si3 V |
Title of publication | Redox-Noninnocent Ligand-Supported Vanadium Catalysts for the Chemoselective Reduction of C═X (X = O, N) Functionalities. |
Authors of publication | Zhang, Guoqi; Wu, Jing; Zheng, Shengping; Neary, Michelle C.; Mao, Jincheng; Flores, Marco; Trovitch, Ryan J.; Dub, Pavel A. |
Journal of publication | Journal of the American Chemical Society |
Year of publication | 2019 |
Journal volume | 141 |
Journal issue | 38 |
Pages of publication | 15230 - 15239 |
a | 10.8649 ± 0.0009 Å |
b | 12.4225 ± 0.001 Å |
c | 13.0617 ± 0.0011 Å |
α | 115.202 ± 0.004° |
β | 96.239 ± 0.004° |
γ | 96.088 ± 0.004° |
Cell volume | 1562.8 ± 0.2 Å3 |
Cell temperature | 130 ± 2 K |
Ambient diffraction temperature | 130 ± 2 K |
Number of distinct elements | 5 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.115 |
Residual factor for significantly intense reflections | 0.059 |
Weighted residual factors for significantly intense reflections | 0.1173 |
Weighted residual factors for all reflections included in the refinement | 0.1524 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.062 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4129019.html
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Users of the data should acknowledge the original authors of the
structural data.