Information card for entry 4129841

Structure parameters

• Formula: C28 H37 Cl N2 O3 Si
• Calculated formula: C28 H37 Cl N2 O3 Si
• SMILES: [Si](OC1=C(C(=O)N2CCCCC2)[C@@H](N(OC1)c1ccccc1)c1ccc(Cl)cc1)(C(C)(C)C)(C)C
• Title of publication: Copper-Catalyzed Divergent Addition Reactions of Enoldiazoacetamides with Nitrones.
• Authors of publication: Cheng, Qing-Qing; Yedoyan, Julietta; Arman, Hadi; Doyle, Michael P.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 1
• Pages of publication: 44 - 47
• a: 6.52 ± 0.004 Å
• b: 18.36 ± 0.01 Å
• c: 12.283 ± 0.007 Å
• α: 90°
• β: 99.174 ± 0.01°
• γ: 90°
• Cell volume: 1451.6 ± 1.5 ų
• Cell temperature: 293 K
• Ambient diffraction temperature: 293 K
• Number of distinct elements: 6
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0925
• Residual factor for significantly intense reflections: 0.0782
• Weighted residual factors for significantly intense reflections: 0.1385
• Weighted residual factors for all reflections included in the refinement: 0.1474
• Goodness-of-fit parameter for all reflections included in the refinement: 1.036
• Diffraction radiation wavelength: 0.71075 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No