Information card for entry 4129954

Structure parameters

• Formula: C24 H30 F6 N3 O3 Rh Sb
• Calculated formula: C24 H30 F6 N3 O3 Rh Sb
• Title of publication: A Stable Coordination Complex of Rh(IV) in an N,O-Donor Environment.
• Authors of publication: Sinha, Shashi B.; Shopov, Dimitar Y.; Sharninghausen, Liam S.; Vinyard, David J.; Mercado, Brandon Q.; Brudvig, Gary W.; Crabtree, Robert H.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2015
• Journal volume: 137
• Journal issue: 50
• Pages of publication: 15692 - 15695
• a: 14.7512 ± 0.001 Å
• b: 33.1199 ± 0.0006 Å
• c: 12.0932 ± 0.0002 Å
• α: 90°
• β: 103.836 ± 0.007°
• γ: 90°
• Cell volume: 5736.8 ± 0.4 ų
• Cell temperature: 93 ± 2 K
• Ambient diffraction temperature: 93 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.064
• Residual factor for significantly intense reflections: 0.0555
• Weighted residual factors for significantly intense reflections: 0.125
• Weighted residual factors for all reflections included in the refinement: 0.1298
• Goodness-of-fit parameter for all reflections included in the refinement: 1.128
• Diffraction radiation wavelength: 1.54187 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No