Information card for entry 4130371

Structure parameters

• Formula: C64.5 H82 Fe N2 O4 Si
• Calculated formula: C64.5 H82 Fe N2 O4 Si
• Title of publication: Activation of 7-Silanorbornadienes by N-Heterocyclic Carbenes: A Selective Way to N-Heterocyclic-Carbene-Stabilized Silylenes.
• Authors of publication: Lutters, Dennis; Severin, Claudia; Schmidtmann, Marc; Müller, Thomas
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 18
• Pages of publication: 6061 - 6067
• a: 22.2976 ± 0.0005 Å
• b: 21.8242 ± 0.0005 Å
• c: 23.9794 ± 0.0005 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 11669 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0693
• Residual factor for significantly intense reflections: 0.045
• Weighted residual factors for significantly intense reflections: 0.0994
• Weighted residual factors for all reflections included in the refinement: 0.1109
• Goodness-of-fit parameter for all reflections included in the refinement: 1.029
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No