Information card for entry 4130784

Structure parameters

• Formula: C254 H205 F48 Fe4 N31 O2 Sb8
• Calculated formula: C254 H205 F38.508 Fe4 N31 O2 Sb6.418
• Title of publication: Pathway-Dependent Post-assembly Modification of an Anthracene-Edged M(II)4L6 Tetrahedron.
• Authors of publication: Ronson, Tanya K.; Pilgrim, Ben S.; Nitschke, Jonathan R.
• Journal of publication: Journal of the American Chemical Society
• Year of publication: 2016
• Journal volume: 138
• Journal issue: 33
• Pages of publication: 10417 - 10420
• a: 22.5576 ± 0.0004 Å
• b: 25.9536 ± 0.0004 Å
• c: 26.6117 ± 0.0004 Å
• α: 102.011 ± 0.001°
• β: 93.562 ± 0.001°
• γ: 100.843 ± 0.001°
• Cell volume: 14883.3 ± 0.4 ų
• Cell temperature: 180 ± 2 K
• Ambient diffraction temperature: 180 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1244
• Residual factor for significantly intense reflections: 0.0973
• Weighted residual factors for significantly intense reflections: 0.306
• Weighted residual factors for all reflections included in the refinement: 0.3355
• Goodness-of-fit parameter for all reflections included in the refinement: 1.368
• Diffraction radiation wavelength: 1.54178 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No